Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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Some specific hazards statements are given in When a test has been selected, follow the detailed directions in that standard for making up the test solution, the preparation of test samples and the finish to be used.
ASTM A Intergranular Corrosion Testing and Analysis
R Baboian, Corrosion Tests and Standards: There is several cause for SCC, Chloride is the leading cause of transgranular cracking or attack. What is your typical turnaround time?
SEP does not require ageing, although it might be required in a specification calling up this standard. ISO is the most rigorous in terms of defining test methods, and says which alloys should use which test methods asttm follows:. Conducting the Tests When a test has been selected, follow the detailed directions in that standard for making up the test solution, the preparation of test samples and the finish to be used. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
Practice A is a rapid a62 examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. If the structure is acceptable no additional testing is required. Test Samples Samples may be rectangular or cylindrical to suit the test ast, but where a bend test is required, it is suggested that the sample be a minimum of mm long.
Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power microscope and a microsection in any suspicious areas.
Intergranular Attack – ASTM A – Colorado-Metallurgical-Services
Just remember that these tests were devised for specific groups of alloys and should not be applied to all CRAs! The effect of post weld surface treatments on the corrosion resistance of super duplex stainless steel welds in sea water Carbon and Sulfur Analysis. Methods B and E are suggested for all grades of series austenitic alloys, while method F is suggested for cast type alloys. Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the asstm be a minimum of mm long.
This method is preferable for chromium depletions and corrosion in intermetallic phases.
Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. The level of corrosion is determined asfm mass loss. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. These practices include five intergranular corrosion tests, namely: The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.
The Tests Table 1 below shows the various methods for four common standards: To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
Some standards require the test sample to be aged prior to testing, to simulate the precipitation that might occur during welding.
The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
Because it can be run quickly for screening, we often run this test first. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.
ASTM G28 does not require samples to be heat treated. This document describes all three of these tests for four common standards, and describes the differences.